APS Logo

Laue Diffraction in the High Pressure Collaborative Access Team (HPCAT).

ORAL

Abstract

Polychromatic beam diffraction technique is a powerful tool to investigate pressure induced processes in-situ and in-operando. Microstructural information including strain, orientation relations, twinning, crystal morphology is available across phase transitions, deformation, chemical processes. Using this information combined with theory, mechanisms and driving forces of such processes can be investigated. Experimental setup specifically optimized for application of high pressure Laue diffraction is available and open for users at HPCAT. Recent case studies including mechanism of Si I to Si II phase transition, pressure induced processes in Cu50Fe50 precipitates and high entropy alloys will be presented.

Publication: D. Popov, N. Velisavljevic, Wenjun Liu, R. Hrubiak, C. Park, and G. Shen. Real time study of grain enlargement in zirconium under room-temperature compression across the a to ? phase transition Sci. Rep. 9, 15712 (2019)<br><br>D. Popov, N. Velisavljevic, and M. Somayazulu. (2019) Mechanisms of Pressure-Induced Phase Transitions by Real-Time Laue Diffraction. Crystals 9, 12: 672<br><br>H. Chen, V. I. Levitas, D. Popov, N. Velisavljevic Novel nanostructure, stress relaxation mechanisms, and crystallography for pressure-induced Si-I ? Si-II phase transformation. Submitted to Nature Communications.<br><br>A. Chatterjee, D. Popov, A. Misra, N. Velisavljevic Compression of Cu50Fe50 precipitates. Manuscript in preparation.

Presenters

  • Dmitry Popov

    HPCAT, X-ray Science Division, Argonne National Laboratory, High-pressure Collaborative Access Team, Advanced Photon Source, Argonne National Laboratory, Lemont, IL 60439, Argonne National Laboratory

Authors

  • Dmitry Popov

    HPCAT, X-ray Science Division, Argonne National Laboratory, High-pressure Collaborative Access Team, Advanced Photon Source, Argonne National Laboratory, Lemont, IL 60439, Argonne National Laboratory

  • Curtis Kenney-Benson

    High-pressure Collaborative Access Team, Advanced Photon Source, Argonne National Laboratory, Lemont, IL 60439, Argonne National Laboratory

  • Arun Bommannavar

    High-pressure Collaborative Access Team, Advanced Photon Source, Argonne National Laboratory, Lemont, IL 60439, Argonne National Laboratory

  • Maddury S Somayazulu

    HPCAT, X-ray Science Division, Argonne National Laboratory, Argonne National Laboratory

  • Nenad Velisavljevic

    Lawrence Livermore Natl Lab