New Soft Matter Soft X-ray Scattering Facility and the Advanced Light Source with Real Time Analysis

POSTER

Abstract

We present the development and first experiments at a new user scattering facility at the Advanced Light Source at Lawrence Berkeley National Laboratory designed to elucidate the structure of polymer thin films, including a number of systems important for understanding organic devices. These experiments utilize enhanced contrast mechanisms available due to resonance effects to gain sensitivity to morphology which other probes and harder X-ray beams cannot probe. We present the development of new characterization and calibration techniques as well as procedures to mitigate the unique problems that come with scattering in this energy range. These allow us to obtain quantitative scattering profiles and thus ensemble morphological information of these devices. In addition, we present a live analysis package which does initial data reduction in real time while scattering data is being collected.

Authors

  • Eliot Gann

    North Carolina State University, Jema Science Inc., North Carolina State University

  • Anthony Young

    Lawrence Berkeley National Laboratory

  • Brian Collins

    North Carolina State University

  • Hongping Yan

    NCSU, North Carolina State University

  • Howard Padmore

    Lawrence Berkeley National Laboratory

  • Harald Ade

    North Carolina State University, NC State University

  • Alexander Hexemer

    Lawerence Berkeley National Laboratory, LBNL, Lawrence Berkeley National Laboratory, Advanced Light Source, Lawrence Berkeley National Laboratory

  • Cheng Wang

    LBNL, Lawrence Berkeley National Laboratory